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Could you tell us what camera and what metering mode you were using? Or were you setting the exposure manually?
hmm, looks too tall for a fill flash ... 10-20 metres?
for a graduated ND the shape is a bit complicated ... it wil leave the top of the building rather dark.
I use Bibble to edit and there is "Fill Light" which is supposed to lighten up dark areas without changing the exposure so I guess I could expose for the sky which would make the structure too dark and lighten it up again using Fill Light.
Does this sound right?